This volume delves into recent innovative approaches and advancements in the dynamic fields of materials engineering and nanotechnology. It offers a comprehensive exploration of diverse topics, ranging from advanced materials synthesis and characterization to nanoscale science and engineering, functional composite materials, and sustainable technologies. Curated from the esteemed 8th International Conference on Material Engineering and Nanotechnology (ICMEN 2024) held in Kuala Lumpur, Malaysia, on September 28th-29th, 2024, this book presents peer reviewed articles authored by experts across various domains of materials engineering and nanotechnology. The significance of these proceedings lies in their profound impact on advancing the collective knowledge and understanding within the scientific community. By disseminating cutting-edge research findings and innovations, this publication serves as a catalyst for collaboration, idea generation, and the expansion of scientific horizons. With its broad scope and relevance, this book is indispensable for materials and nanotechnology engineers, scholars, and researchers across science, technology, and engineering disciplines.